9QK6
X-ray crystal structure of SlPYL1-FeruloylPhenylalanine complex
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALBA BEAMLINE XALOC |
| Synchrotron site | ALBA |
| Beamline | XALOC |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-10-25 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.979 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 90.042, 90.042, 50.997 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 77.980 - 1.750 |
| R-factor | 0.2041 |
| Rwork | 0.202 |
| R-free | 0.24470 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.348 |
| Data reduction software | autoPROC |
| Data scaling software | autoPROC |
| Refinement software | PHENIX (1.21.2_5419) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 77.980 | 1.813 |
| High resolution limit [Å] | 1.750 | 1.750 |
| Number of reflections | 24319 | 2407 |
| <I/σ(I)> | 3.46 | |
| Completeness [%] | 99.9 | |
| Redundancy | 1.34 | |
| CC(1/2) | 0.923 | 0.923 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | MICROBATCH | 7 | 295 | 3.5 M ammonium sulfate pH 7.0 |
