9QIU
Crystal structure of YTHDF2 in complex with compound 13 (AI-DF2-56)
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-02-03 |
| Detector | DECTRIS PILATUS 2M-F |
| Wavelength(s) | 1 |
| Spacegroup name | P 65 |
| Unit cell lengths | 79.440, 79.440, 115.800 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 44.300 - 2.460 |
| R-factor | 0.2252 |
| Rwork | 0.222 |
| R-free | 0.27900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.892 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.21.1.5286) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.610 |
| High resolution limit [Å] | 2.450 | 2.460 |
| Number of reflections | 15021 | 2375 |
| <I/σ(I)> | 9.48 | |
| Completeness [%] | 99.7 | |
| Redundancy | 6.85 | |
| CC(1/2) | 0.994 | 0.834 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 277.15 | 2.025 M Ammonium sulfate, 0.1 M Sodium citrate tribasic pH 5.2 |
