9PSK

In situ MicroED structure of IL-33 activated human eosinophil major basic protein-1

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	31.700, 59.460, 60.270
Unit cell angles	90.00, 91.74, 90.00

Refinement procedure

Resolution	31.690 - 3.180
R-factor	0.269
Rwork	0.261
R-free	0.33960
RMSD bond length	0.002
RMSD bond angle	0.453
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHENIX
Refinement software	PHENIX (1.21.1_5286)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	31.690	31.690	3.640
High resolution limit [Å]	3.180	4.590	3.180
Rmerge	0.547	0.414	1.231
Rmeas	0.581	0.438	1.319
Total number of observations	61440
Number of reflections	7190	2445	2245
<I/σ(I)>	3.63	5.16	1.95
Completeness [%]	97.2
CC(1/2)	0.879	0.889	0.420