Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-12-18 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.9999 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 99.139, 137.018, 38.524 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 80.340 - 1.280 |
| R-factor | 0.15308 |
| Rwork | 0.151 |
| R-free | 0.19456 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.826 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | REFMAC |
| Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 80.340 | 1.530 |
| High resolution limit [Å] | 1.280 | 1.280 |
| Rmeas | 0.032 | 0.522 |
| Number of reflections | 135419 | 55554 |
| <I/σ(I)> | 19.96 | |
| Completeness [%] | 99.5 | 99.6 |
| Redundancy | 5 | 5 |
| CC(1/2) | 1.000 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7.5 | 285 | 19% (w/v) PEG3350, 0.17M Magnesium formate |
