9PHK

[19-7B G|T] 19 bp tensegrity triangle that propagates via blunt-end stacking with G stacking on T at the interface

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-12-11
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1.007430
Spacegroup name	I 41 3 2
Unit cell lengths	157.208, 157.208, 157.208
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	33.520 - 6.010
R-factor	0.1355
Rwork	0.132
R-free	0.25390
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.682
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	PHASER
Refinement software	PHENIX (1.21.2_5419)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	64.180	64.180	6.505
High resolution limit [Å]	6.010	10.747	6.011
Number of reflections	948	188	189
<I/σ(I)>	52.8
Completeness [%]	100.0
Redundancy	70.3
CC(1/2)	1.000	1.000	0.993

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	100 mM MOPS, 1.25 M magnesium sulfate