9OZV

Structure of the self-association domain of LDB2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX2
Synchrotron site	Australian Synchrotron
Beamline	MX2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2023-12-08
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.95373
Spacegroup name	P 1 21 1
Unit cell lengths	38.628, 95.876, 49.129
Unit cell angles	90.00, 108.02, 90.00

Refinement procedure

Resolution	46.720 - 2.590
R-factor	0.2755
Rwork	0.268
R-free	0.34140
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.004
RMSD bond angle	0.717
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.940	2.700
High resolution limit [Å]	2.590	2.590
Number of reflections	10574	10574
<I/σ(I)>	6.4
Completeness [%]	99.1
Redundancy	1.9
CC(1/2)	0.998	0.999

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	Ammonium sulfate, HEPES, PEG 8000, MPD