9OSM

[4,8,7-2] Shifted tensegrity triangle with an (arm,center,arm) distribution of (4,8,7) base pairs and 2 nt sticky ends complexing calcium

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2023-05-13
Detector	DECTRIS EIGER X 9M
Wavelength(s)	0.92010
Spacegroup name	H 3
Unit cell lengths	111.704, 111.704, 67.674
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	39.350 - 2.930
R-factor	0.2323
Rwork	0.229
R-free	0.29090
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	0.828
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	PHASER
Refinement software	PHENIX (1.21.2_5419)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	55.852	55.852	3.258
High resolution limit [Å]	2.930	9.560	2.930
Number of reflections	3522	195	196
<I/σ(I)>	10.1
Completeness [%]	76.5
Redundancy	8.5
CC(1/2)	0.999	0.999	0.748

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	100 mM MOPS, 1.25 M magnesium sulfate