9NQA
[0,9,10-2] Shifted tensegrity triangle with an (arm,center,arm) distribution of (0,9,10) base pairs and 2 nt sticky ends containing a semi-junction
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-11-13 |
| Detector | DECTRIS EIGER X 9M |
| Wavelength(s) | 1.000000 |
| Spacegroup name | H 3 |
| Unit cell lengths | 102.862, 102.862, 104.207 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 34.740 - 5.470 |
| R-factor | 0.1385 |
| Rwork | 0.137 |
| R-free | 0.17310 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.811 |
| Data reduction software | autoPROC |
| Data scaling software | STARANISO |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 67.712 | 67.712 | 6.037 |
| High resolution limit [Å] | 5.469 | 10.334 | 5.469 |
| Number of reflections | 1219 | 202 | 203 |
| <I/σ(I)> | 6.2 | ||
| Completeness [%] | 89.0 | ||
| Redundancy | 10.2 | ||
| CC(1/2) | 0.999 | 0.999 | 0.116 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 100 mM MOPS, 1.25 M magnesium sulfate |
