9NNY

[4,7,8-2] Shifted tensegrity triangle with an (arm,center,arm) distribution of (4,7,8) base pairs and 2 nt sticky ends, with hexagonal symmetry

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-10-16
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1.00001
Spacegroup name	P 63
Unit cell lengths	126.120, 126.120, 64.570
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	36.410 - 4.440
R-factor	0.1974
Rwork	0.196
R-free	0.22770
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.874
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	PHASER
Refinement software	PHENIX (1.21.2_5419)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	63.060	63.060	4.838
High resolution limit [Å]	4.440	12.007	4.440
Number of reflections	2831	203	203
<I/σ(I)>	8.5
Completeness [%]	89.5
Redundancy	17.3
CC(1/2)	0.999	0.999	0.472

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	100 mM MOPS, 1.25 M magnesium sulfate