9NM9

[2T8-SiO2] Hexagonal tensegrity triangle lattice coated in silica

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS-II BEAMLINE 17-ID-2
Synchrotron site	NSLS-II
Beamline	17-ID-2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-10-05
Detector	DECTRIS EIGER2 X 16M
Wavelength(s)	0.97856
Spacegroup name	P 63
Unit cell lengths	130.501, 130.501, 52.840
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.800 - 6.560
R-factor	0.1992
Rwork	0.199
R-free	0.20510
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.913
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	19.802	19.802	7.528
High resolution limit [Å]	6.560	10.525	6.563
Number of reflections	878	220	219
<I/σ(I)>	7.7
Completeness [%]	89.7
Redundancy	9.7
CC(1/2)	0.998	0.999	0.492

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8	293	100 mM MOPS, 1.25 M magnesium sulfate