9NM7

[2T7-SiO2] Rhombohedral tensegrity triangle lattice coated in silica

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS-II BEAMLINE 17-ID-1
Synchrotron site	NSLS-II
Beamline	17-ID-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2023-05-13
Detector	DECTRIS EIGER2 X 16M
Wavelength(s)	0.92010
Spacegroup name	H 3
Unit cell lengths	107.532, 107.532, 88.412
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.240 - 4.760
R-factor	0.2517
Rwork	0.247
R-free	0.34460
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.982
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	19.240	19.236	5.493
High resolution limit [Å]	4.756	9.743	4.756
Number of reflections	1330	191	190
<I/σ(I)>	7.4
Completeness [%]	83.5
Redundancy	5.5
CC(1/2)	0.999	0.999	0.524

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8	293	100 mM MOPS, 1.25 M magnesium sulfate