9NEW
[1,8,11-1] Shifted tensegrity triangle with an (arm,center,arm) distribution of (1,8,11) base pairs and 1 nt sticky ends
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-03-19 |
| Detector | DECTRIS EIGER X 9M |
| Wavelength(s) | 0.991870 |
| Spacegroup name | P 63 |
| Unit cell lengths | 132.686, 132.686, 50.985 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 66.340 - 6.910 |
| R-factor | 0.2812 |
| Rwork | 0.276 |
| R-free | 0.36940 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.757 |
| Data reduction software | autoPROC |
| Data scaling software | STARANISO |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 66.343 | 66.343 | 8.065 |
| High resolution limit [Å] | 6.910 | 11.835 | 6.913 |
| Number of reflections | 757 | 189 | 189 |
| <I/σ(I)> | 8.4 | ||
| Completeness [%] | 88.1 | ||
| Redundancy | 19.2 | ||
| CC(1/2) | 0.996 | 0.996 | 0.212 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 100 mM MOPS, 1.25 M magnesium sulfate |
