9NC5
[4,14,11-2] Shifted tensegrity triangle with an (arm,center,arm) distribution of (4,14,11) base pairs and 2 nt sticky ends
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-11-13 |
| Detector | DECTRIS EIGER X 9M |
| Wavelength(s) | 1.000000 |
| Spacegroup name | H 3 |
| Unit cell lengths | 164.619, 164.619, 107.526 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 38.060 - 7.370 |
| R-factor | 0.165 |
| Rwork | 0.159 |
| R-free | 0.22060 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.934 |
| Data reduction software | autoPROC |
| Data scaling software | STARANISO |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 85.846 | 85.846 | 8.408 |
| High resolution limit [Å] | 7.370 | 14.399 | 7.372 |
| Number of reflections | 1157 | 196 | 194 |
| <I/σ(I)> | 10.1 | ||
| Completeness [%] | 83.6 | ||
| Redundancy | 8.7 | ||
| CC(1/2) | 0.999 | 0.999 | 0.420 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 100 mM MOPS, 1.25 M magnesium sulfate |
