9MNV
Co-MAHF-9 A8Y Metal Alpha-Helix Framework
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-12-19 |
| Detector | RIGAKU HyPix-3000 |
| Wavelength(s) | 1.54184 |
| Spacegroup name | P 1 |
| Unit cell lengths | 10.227, 16.303, 20.648 |
| Unit cell angles | 92.69, 103.39, 108.10 |
Refinement procedure
| Resolution | 19.920 - 0.800 |
| R-factor | 0.113 |
| Rwork | 0.113 |
| R-free | 0.11440 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.528 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.21.2_5419) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.920 | 0.829 |
| High resolution limit [Å] | 0.800 | 0.800 |
| Number of reflections | 12241 | 995 |
| <I/σ(I)> | 26.67 | |
| Completeness [%] | 94.6 | |
| Redundancy | 4.2 | |
| CC(1/2) | 0.995 | 0.790 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | SLOW COOLING | 298 | water, acetonitrile, cobalt acetate, sodium hydroxide, methanol |
