Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-11-11 |
| Detector | DECTRIS EIGER2 X 9M |
| Wavelength(s) | 1 |
| Spacegroup name | P 1 |
| Unit cell lengths | 72.580, 82.410, 83.440 |
| Unit cell angles | 116.05, 97.71, 98.68 |
Refinement procedure
| Resolution | 73.030 - 1.660 |
| R-factor | 0.202 |
| Rwork | 0.201 |
| R-free | 0.22300 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.000 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.7 (20-MAY-2020)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 73.030 | 1.830 |
| High resolution limit [Å] | 1.660 | 1.660 |
| Number of reflections | 202912 | 10634 |
| <I/σ(I)> | 13.9 | 1.7 |
| Completeness [%] | 81.1 | |
| Redundancy | 1.8 | |
| CC(1/2) | 0.999 | 0.615 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 295 | 0.2 M magnesium formate, 20% (w/v) PEG 3,350, 0.1 M TCEP |
