Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PETRA III, DESY BEAMLINE P11 |
| Synchrotron site | PETRA III, DESY |
| Beamline | P11 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-05-06 |
| Detector | DECTRIS EIGER2 X 16M |
| Wavelength(s) | 1.03320 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 85.882, 85.882, 346.510 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 49.780 - 2.350 |
| R-factor | 0.20795 |
| Rwork | 0.205 |
| R-free | 0.26194 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.446 |
| Data reduction software | Aimless |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.780 | 2.420 |
| High resolution limit [Å] | 2.350 | 2.350 |
| Rmerge | 0.084 | 1.877 |
| Number of reflections | 55489 | 4465 |
| <I/σ(I)> | 26.1 | 2.3 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 26.3 | 25.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.15 M Ammonium sulfate,0.1 M TRIS pH 7.8, 15% w/v PEG 4000 |
