9LZX

Crystal structure of the OTU domain of OTULIN in complex with 11B6

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-04-27
Detector	RIGAKU HyPix-6000HE
Wavelength(s)	1.54
Spacegroup name	P 21 21 21
Unit cell lengths	45.176, 72.535, 94.062
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	23.720 - 2.000
R-factor	0.1963
Rwork	0.193
R-free	0.25140
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.870
Data scaling software	SCALA
Phasing software	MOLREP
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	23.720	2.050
High resolution limit [Å]	2.000	2.000
Rmerge	0.096	0.367
Number of reflections	21514	1580
<I/σ(I)>	11.3
Completeness [%]	99.8
Redundancy	4.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	PEG 3350,MES,magnesium chloride