9LTF

Crystal structure of mSTING-TTB

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-08-20
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.987
Spacegroup name	P 31 2 1
Unit cell lengths	79.611, 79.611, 49.909
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	34.470 - 1.920
R-factor	0.2003
Rwork	0.198
R-free	0.23930
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.106
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((1.19.2_4158: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	34.470	1.990
High resolution limit [Å]	1.920	1.920
Number of reflections	14210	14094
<I/σ(I)>	33.17
Completeness [%]	99.1
Redundancy	18.8
CC(1/2)	0.997	0.860

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	0.5 M Sodium citrate pH5.5, 16% PEG4000