9LNV

Crystal structure of T2R-TTL-YQVB6 Complex

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NFPSS BEAMLINE BL19U1
Synchrotron site	NFPSS
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-12-10
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97861
Spacegroup name	P 21 21 21
Unit cell lengths	105.211, 156.467, 184.705
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	91.420 - 2.670
R-factor	0.2214
Rwork	0.218
R-free	0.28770
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond angle	17.288
Data reduction software	xia2
Data scaling software	XDS
Phasing software	PHENIX
Refinement software	PHENIX ((???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	119.390	2.720
High resolution limit [Å]	2.670	2.670
Number of reflections	87167	4276
<I/σ(I)>	4.2
Completeness [%]	100.0
Redundancy	13.2
CC(1/2)	0.959	0.481

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	6% PEG, 5% glycerol, 0.1 M MES, 30 mM CaCl2, 30 mM MgCl2, pH 6.7