9LNL

Crystal structure of T2R-TTL-YQVB15 complex

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-12-10
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97861
Spacegroup name	P 21 21 21
Unit cell lengths	105.300, 156.420, 184.860
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	53.180 - 2.850
R-factor	0.2014
Rwork	0.198
R-free	0.27740
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond angle	18.269
Data reduction software	xia2
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.21_5207: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	53.190	2.900
High resolution limit [Å]	2.850	2.850
Number of reflections	71704	3531
<I/σ(I)>	6.4
Completeness [%]	99.7
Redundancy	13.4
CC(1/2)	0.982	0.497

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	6% PEG, 5% glycerol, 0.1 M MES, 30 mM CaCl2, 30 mM MgCl2, pH 6.7