9L9S

The crystal structure of UG15

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-12-12
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97855
Spacegroup name	I 41 2 2
Unit cell lengths	198.586, 198.586, 349.674
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	35.105 - 3.305
R-factor	0.2606
Rwork	0.260
R-free	0.28360
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	0.991
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHASER
Refinement software	PHENIX ((1.15.2_3472: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	3.360
High resolution limit [Å]	3.300	3.300
Number of reflections	52351	2560
<I/σ(I)>	16.6
Completeness [%]	99.7
Redundancy	26.9
CC(1/2)	0.972	0.754

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	6% PEG 10000, 5%n-propanol, 0.1M MES(pH6.2)