Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL02U1 |
| Synchrotron site | SSRF |
| Beamline | BL02U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-05-26 |
| Detector | DECTRIS EIGER2 S 9M |
| Wavelength(s) | 0.97918 |
| Spacegroup name | P 1 |
| Unit cell lengths | 58.163, 58.406, 95.479 |
| Unit cell angles | 74.45, 88.13, 76.18 |
Refinement procedure
| Resolution | 91.930 - 3.050 |
| R-factor | 0.29252 |
| Rwork | 0.290 |
| R-free | 0.34030 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.011 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 91.930 | 3.260 |
| High resolution limit [Å] | 3.050 | 3.050 |
| Rmerge | 0.147 | 0.508 |
| Rmeas | 0.173 | 0.603 |
| Rpim | 0.090 | 0.320 |
| Number of reflections | 22166 | 4016 |
| <I/σ(I)> | 5.7 | 2 |
| Completeness [%] | 99.0 | 98.3 |
| Redundancy | 3.5 | |
| CC(1/2) | 0.989 | 0.863 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 291.15 | 0.05 M KH2PO4, pH 7.0, 25% PEG3350 |
