9KPP

Crystal structure of FrazP2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL10U2
Synchrotron site	SSRF
Beamline	BL10U2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-05-01
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.9785
Spacegroup name	P 1
Unit cell lengths	39.150, 52.960, 54.020
Unit cell angles	117.68, 104.06, 93.26

Refinement procedure

Resolution	26.480 - 1.850
R-factor	0.1659
Rwork	0.164
R-free	0.19680
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.025
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.19.2_4158: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	26.480	1.916
High resolution limit [Å]	1.850	1.850
Number of reflections	29682	2955
<I/σ(I)>	2.05
Completeness [%]	95.2
Redundancy	2.05
CC(1/2)	0.998	0.896

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.5	293	0.085 M Sodium acetate trihydrate (pH 4.6), 25.5 % PEG 4000, 0.17 M Ammonium acetate and 15 % Glycerol