Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-12-21 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9786 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 127.610, 51.090, 41.750 |
| Unit cell angles | 90.00, 96.30, 90.00 |
Refinement procedure
| Resolution | 24.631 - 1.800 |
| R-factor | 0.188810488445 |
| Rwork | 0.187 |
| R-free | 0.22249 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.189 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 24.631 | 1.840 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 1.005 | |
| Number of reflections | 24877 | 1481 |
| <I/σ(I)> | 15.9 | |
| Completeness [%] | 99.8 | |
| Redundancy | 6.5 | |
| CC(1/2) | 0.999 | 0.872 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M sodium acetate trihydrate pH 4.5, 3.0 M sodium chloride |
