Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL44XU |
| Synchrotron site | SPring-8 |
| Beamline | BL44XU |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-06-19 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.9 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 51.536, 77.510, 111.271 |
| Unit cell angles | 90.00, 92.38, 90.00 |
Refinement procedure
| Resolution | 42.890 - 1.550 |
| R-factor | 0.18991 |
| Rwork | 0.189 |
| R-free | 0.21142 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.947 |
| Data reduction software | xia2 |
| Refinement software | REFMAC (5) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 42.890 | 1.580 |
| High resolution limit [Å] | 1.550 | 1.550 |
| Number of reflections | 123365 | 4844 |
| <I/σ(I)> | 7.2 | |
| Completeness [%] | 97.3 | |
| Redundancy | 3.2 | |
| CC(1/2) | 0.948 | 0.656 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M Tris-HCl pH 8.0, 20%(w/v) PEG6000, and 0.2 M CaCl2 |
