9JW4

Crystal structure of OsSPS3 complexed with YH24785

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-06-22
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.979230
Spacegroup name	P 21 21 21
Unit cell lengths	56.265, 89.669, 128.464
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.660 - 1.760
R-factor	0.2137
Rwork	0.212
R-free	0.25260
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.765
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.21.1_5286: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.660	1.823
High resolution limit [Å]	1.760	1.760
Number of reflections	65191	6425
<I/σ(I)>	23.5
Completeness [%]	98.1
Redundancy	10.165
CC(1/2)	0.999	0.879

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	PEG3350, Bis-Tris, Ammonium sulfate