9JV9

Crystal structure of OsSPS3 complexed with YH24272

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL10U2
Synchrotron site	SSRF
Beamline	BL10U2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-05-19
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.979183
Spacegroup name	P 21 21 21
Unit cell lengths	56.673, 90.179, 128.586
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.712 - 1.655
R-factor	0.1944
Rwork	0.193
R-free	0.22540
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.720
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.16_3549: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	38.712	1.714
High resolution limit [Å]	1.655	1.655
Number of reflections	76920	7380
<I/σ(I)>	17.43
Completeness [%]	96.9
Redundancy	10.423
CC(1/2)	0.999	0.817

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	PEG3350, Bis-Tris, Ammonium sulfate