9JV5

Crystal structure of OsSPS3 complexed with YH24287

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL10U2
Synchrotron site	SSRF
Beamline	BL10U2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-05-19
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.979183
Spacegroup name	P 21 21 21
Unit cell lengths	56.765, 90.378, 128.545
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	42.547 - 2.098
R-factor	0.2136
Rwork	0.211
R-free	0.25490
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.830
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.16_3549: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.550	2.173
High resolution limit [Å]	2.098	2.098
Number of reflections	39413	3884
<I/σ(I)>	11.55
Completeness [%]	99.7
Redundancy	10.148
CC(1/2)	0.998	0.836

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	PEG3350, Bis-Tris, Ammonium sulfate