9JSC

Crystal structure of OsSPS3 complexed with YH24532

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL10U2
Synchrotron site	SSRF
Beamline	BL10U2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-04-14
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.987
Spacegroup name	P 21 21 21
Unit cell lengths	56.726, 90.314, 128.463
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	42.519 - 1.994
R-factor	0.224
Rwork	0.221
R-free	0.27800
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.839
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.16_3549: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.520	2.065
High resolution limit [Å]	1.994	1.994
Number of reflections	43406	4167
<I/σ(I)>	16.38
Completeness [%]	93.0
Redundancy	10.42
CC(1/2)	0.999	0.830

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	PEG3350, Ammonium sulfate, Bis-Tris