9JS8

Crystal structure of OsSPS3 complexed with YH24508

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL10U2
Synchrotron site	SSRF
Beamline	BL10U2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-04-14
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.987
Spacegroup name	P 21 21 21
Unit cell lengths	56.808, 90.346, 128.342
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	29.319 - 1.829
R-factor	0.194
Rwork	0.192
R-free	0.22430
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.760
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.16_3549: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	29.320	1.894
High resolution limit [Å]	1.829	1.829
Number of reflections	59015	5740
<I/σ(I)>	11.32
Completeness [%]	99.7
Redundancy	10.28
CC(1/2)	0.995	0.631

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	PEG3350, Bis-Tris, Ammonium sulfate