Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-17A |
| Synchrotron site | Photon Factory |
| Beamline | BL-17A |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-05-14 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.98 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 51.518, 78.201, 111.144 |
| Unit cell angles | 90.00, 92.64, 90.00 |
Refinement procedure
| Resolution | 63.930 - 1.390 |
| R-factor | 0.16632 |
| Rwork | 0.165 |
| R-free | 0.18919 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.012 |
| RMSD bond angle | 2.042 |
| Data reduction software | DIALS |
| Data scaling software | Aimless |
| Phasing software | REFMAC |
| Refinement software | REFMAC (5.8.0425) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 63.930 | 1.410 |
| High resolution limit [Å] | 1.390 | 1.390 |
| Rmerge | 0.066 | 0.970 |
| Rmeas | 0.072 | 1.116 |
| Rpim | 0.028 | 0.537 |
| Number of reflections | 164006 | 4569 |
| <I/σ(I)> | 10.9 | 1.2 |
| Completeness [%] | 92.7 | |
| Redundancy | 6.3 | |
| CC(1/2) | 0.998 | 0.582 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M Tris-HCl pH 8.0, 20%(w/v) PEG6000, and 0.2 M CaCl2 |
