9JJ5

CDK2 and its inhibitor DC56

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-11-26
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.97853
Spacegroup name	P 21 21 21
Unit cell lengths	53.593, 71.868, 71.896
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	42.970 - 1.710
R-factor	0.2039
Rwork	0.200
R-free	0.24420
Structure solution method	SIRAS
RMSD bond angle	8.200
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.970	1.740
High resolution limit [Å]	1.710	1.710
Rmerge	0.032	0.406
Number of reflections	22390	277
<I/σ(I)>	41.8
Completeness [%]	99.5
Redundancy	10.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		289	PEG3350,Hepes 7.4