9JGP

Structure of Pd ions bound to human heavy chain ferritin nanocage.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL02U1
Synchrotron site	SSRF
Beamline	BL02U1
Temperature [K]	93
Detector technology	PIXEL
Collection date	2022-09-16
Detector	DECTRIS EIGER2 S 9M
Wavelength(s)	0.979183
Spacegroup name	F 4 3 2
Unit cell lengths	183.700, 183.700, 183.700
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.620 - 1.530
R-factor	0.1733
Rwork	0.173
R-free	0.18450
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	xia2
Data scaling software	xia2
Phasing software	PHENIX
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.620	1.585
High resolution limit [Å]	1.530	1.530
Rmerge	0.237	2.943
Rmeas	0.239	2.966
Number of reflections	40487	3968
<I/σ(I)>	15.52	2.2
Completeness [%]	100.0
Redundancy	76.6
CC(1/2)	0.998	0.775

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	9	283	2 M MgCl2, 0.1 M Bicine, pH 9.0