Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 2 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-12-10 |
| Detector | DECTRIS EIGER X 9M |
| Wavelength(s) | 0.987 |
| Spacegroup name | I 1 2 1 |
| Unit cell lengths | 101.607, 114.919, 104.249 |
| Unit cell angles | 90.00, 103.12, 90.00 |
Refinement procedure
| Resolution | 46.830 - 3.150 |
| R-factor | 0.1925 |
| Rwork | 0.190 |
| R-free | 0.25828 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 8j2v |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (Refmac5) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.830 | 3.260 |
| High resolution limit [Å] | 3.150 | 3.150 |
| Number of reflections | 19895 | 3327 |
| <I/σ(I)> | 5.2 | |
| Completeness [%] | 97.5 | |
| Redundancy | 6.9 | |
| CC(1/2) | 0.990 | 0.460 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.2 M Lithium sulfate, 0.1 M Tris pH 8.5, 30% w/vPEG 4000 |
