9J8G

mouse zbp1 hybrid complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-05-11
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97907
Spacegroup name	P 65 2 2
Unit cell lengths	63.381, 63.381, 71.150
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	43.460 - 1.800
R-factor	0.2025
Rwork	0.201
R-free	0.23440
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.035
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.21rc1_4924: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	43.460	1.940
High resolution limit [Å]	1.800	1.800
Rmerge	0.091	0.839
Number of reflections	14810	1580
<I/σ(I)>	16.17
Completeness [%]	99.9
Redundancy	16.7
CC(1/2)	0.999	0.811

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		278	PEG 4000