Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-01-16 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.97853 |
| Spacegroup name | P 1 |
| Unit cell lengths | 47.030, 61.447, 64.716 |
| Unit cell angles | 68.48, 88.73, 67.79 |
Refinement procedure
| Resolution | 37.450 - 1.800 |
| R-factor | 0.223 |
| Rwork | 0.221 |
| R-free | 0.25480 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3uvm |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.073 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.21rc1_4924: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 37.450 | 1.620 |
| High resolution limit [Å] | 1.600 | 1.600 |
| Rmerge | 0.168 | 0.502 |
| Number of reflections | 155092 | 5002 |
| <I/σ(I)> | 4.48 | |
| Completeness [%] | 95.0 | |
| Redundancy | 3.5 | |
| CC(1/2) | 0.966 | 0.857 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 289 | Bis-tris pH 5.5 25% PEG 4000 |
