9IXS

Crystal structure of TEAD3 YAP binding domain with compound 1

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	100
Detector technology	CCD
Collection date	2022-07-14
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.97
Spacegroup name	P 21 21 21
Unit cell lengths	46.280, 102.650, 149.530
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	29.080 - 2.910
R-factor	0.2173
Rwork	0.211
R-free	0.27520
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.009
RMSD bond angle	1.277
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	29.080	3.014
High resolution limit [Å]	2.910	2.910
Rmerge	0.054	0.388
Number of reflections	16269	1580
<I/σ(I)>	11.9	1.95
Completeness [%]	99.7
Redundancy	2
CC(1/2)	0.996	0.773

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		300	0.1M HEPES pH 7.5, 0.2M Ammonium acetate, 18% PEG 3350