9IVI

Crystal structure of AsfvPrimPol N-terminal domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	100
Detector technology	CCD
Collection date	2021-11-30
Detector	MAR CCD 300 mm
Wavelength(s)	1.5418
Spacegroup name	P 1 21 1
Unit cell lengths	43.712, 72.910, 78.132
Unit cell angles	90.00, 94.97, 90.00

Refinement procedure

Resolution	37.410 - 2.200
Rwork	0.191
R-free	0.25500
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX (1.2.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.240
High resolution limit [Å]	2.200	2.200
Number of reflections	22929	1520
<I/σ(I)>	96
Completeness [%]	95.2
Redundancy	3.6
CC(1/2)	0.982	0.708

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	BisTris propane, PEG 3350, Ammonium sulfate