9IQZ

phage HY126 glycosyltransferase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2023-10-13
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.979
Spacegroup name	P 21 21 21
Unit cell lengths	70.120, 82.720, 139.670
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.950 - 2.610
R-factor	0.1984
Rwork	0.196
R-free	0.24790
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.025
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHENIX
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.950	2.720
High resolution limit [Å]	2.610	2.610
Rmerge	0.085
Number of reflections	25518	3048
<I/σ(I)>	24.3
Completeness [%]	99.9
Redundancy	13
CC(1/2)	0.999	0.961

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		289	0.2M Ammonium chloride; 20% w/v polyethylene glycol 3350