9INS

MONOVALENT CATION BINDING IN CUBIC INSULIN CRYSTALS

Experimental procedure

Spacegroup name	I 21 3
Unit cell lengths	78.900, 78.900, 78.900
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 1.700
R-factor	0.178
RMSD bond length	0.013
RMSD bond angle	0.036
Refinement software	PROLSQ

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	bovine insulin	15 (mg/ml)
2	1	1	sodium phosphate	0.018 (M)
3	1	1	sodium-EDTA	0.01 (M)	pH10.5
4	1	2	sodium phosphate	0.15 (M)
5	1	2	sodium-EDTA	0.01 (M)
6	1	2	xylene	0.5 (%(w/v))	pH9.2