9IK7

Human Serum Albumin crystallized with T4, pH 7.5

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-06-14
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.97946
Spacegroup name	P 1 21 1
Unit cell lengths	59.634, 88.217, 59.724
Unit cell angles	90.00, 103.86, 90.00

Refinement procedure

Resolution	19.960 - 1.970
R-factor	0.2028
Rwork	0.201
R-free	0.24530
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.011
RMSD bond angle	1.717
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.960	2.020
High resolution limit [Å]	1.970	1.970
Rmerge	0.099	0.889
Number of reflections	42419	2973
<I/σ(I)>	11
Completeness [%]	99.8
Redundancy	7.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG