9IK6

Human Serum Albumin crystallized with T4, pH 6.5

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-06-14
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.97946
Spacegroup name	P 1 21 1
Unit cell lengths	59.965, 88.964, 60.447
Unit cell angles	90.00, 104.11, 90.00

Refinement procedure

Resolution	19.910 - 1.690
R-factor	0.1966
Rwork	0.196
R-free	0.23450
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.020
RMSD bond angle	1.769
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.910	1.720
High resolution limit [Å]	1.690	1.690
Rmerge	0.075	0.858
Number of reflections	68111	3601
<I/σ(I)>	12.3
Completeness [%]	99.0
Redundancy	7.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG