9IK3

Human Serum Albumin crystallized with T4, pH 7.5

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-06-14
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.97946
Spacegroup name	P 1 21 1
Unit cell lengths	59.473, 88.392, 59.641
Unit cell angles	90.00, 103.77, 90.00

Refinement procedure

Resolution	19.990 - 2.310
R-factor	0.2259
Rwork	0.222
R-free	0.27060
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.004
RMSD bond angle	0.798
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.990	2.390
High resolution limit [Å]	2.310	2.310
Rmerge	0.118	0.759
Number of reflections	26058	2563
<I/σ(I)>	9.5
Completeness [%]	98.8
Redundancy	7.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG