9I8O

Beta-Catenin R4 with Compound 1

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PETRA III, DESY BEAMLINE P11
Synchrotron site	PETRA III, DESY
Beamline	P11
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-05-21
Detector	DECTRIS EIGER2 X 16M
Wavelength(s)	0.976254
Spacegroup name	P 43 21 2
Unit cell lengths	98.070, 98.070, 232.900
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	90.380 - 2.650
R-factor	0.2164
Rwork	0.212
R-free	0.30539
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	1.302
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	REFMAC (5.8.0419)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	90.380	2.980
High resolution limit [Å]	2.650	2.650
Number of reflections	17407	872
<I/σ(I)>	20.8
Completeness [%]	93.9
Redundancy	25.9
CC(1/2)	1.000	0.663

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.14 M Ammonium acetate, 0.7 M MES pH 6.5, 21% Glycerol ethoxylate