9I2A

FdC of Rhodobacter capsulatus

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID30B
Synchrotron site	ESRF
Beamline	ID30B
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-04-18
Detector	DECTRIS EIGER2 X 9M
Wavelength(s)	0.8731
Spacegroup name	P 21 21 21
Unit cell lengths	45.870, 45.830, 85.300
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.340 - 1.700
R-factor	0.1894
Rwork	0.177
R-free	0.18420
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.004
RMSD bond angle	0.550
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.21_5207: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	24.170	1.690
High resolution limit [Å]	1.600	1.600
Number of reflections	24473	3519
<I/σ(I)>	15
Completeness [%]	100.0
Redundancy	12.5
CC(1/2)	0.999	0.887

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		277.15	0,1 M Tris 8 20 % w/v SOKALAN PA 25 CL in anoxic environment