9HRX

The RSL - pctx complex, H32 form

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 2
Synchrotron site	SOLEIL
Beamline	PROXIMA 2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2023-11-11
Detector	DECTRIS EIGER X 9M
Wavelength(s)	0.98
Spacegroup name	H 3 2
Unit cell lengths	45.893, 45.893, 421.816
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	37.190 - 1.490
R-factor	0.1823
Rwork	0.181
R-free	0.20630
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.004
RMSD bond angle	1.148
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	39.057	1.520
High resolution limit [Å]	1.490	1.490
Rmerge	0.075	0.307
Rmeas	0.077	0.321
Rpim	0.018	0.089
Number of reflections	28854	1339
<I/σ(I)>	24.9	6.5
Completeness [%]	99.8	95.4
Redundancy	17.1
CC(1/2)	0.999	0.955

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.8	293	20% PEG 3350, 0.2 M zinc acetate, 0.1 M Imidazole pH 7.8