9HML
KIR2DL1 bound to RIFIN PfKE01_040007400
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-09-23 |
| Detector | DECTRIS EIGER2 XE 16M |
| Wavelength(s) | 0.976246 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 97.171, 97.171, 109.202 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 28.050 - 2.171 |
| R-factor | 0.2219 |
| Rwork | 0.221 |
| R-free | 0.23190 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.960 |
| Data reduction software | DIALS |
| Data scaling software | DIALS |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.10.4) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 84.150 | 2.210 |
| High resolution limit [Å] | 2.170 | 2.170 |
| Rpim | 0.028 | |
| Number of reflections | 32044 | 1596 |
| <I/σ(I)> | 15.3 | |
| Completeness [%] | 100.0 | |
| Redundancy | 20.3 | |
| CC(1/2) | 0.999 | 0.404 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1M sodium Malonate pH 4.6, 14% PEG 3,350 |
