Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 2 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-03-06 |
| Detector | DECTRIS EIGER X 9M |
| Wavelength(s) | 0.98011 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 67.209, 86.934, 82.466 |
| Unit cell angles | 90.00, 95.24, 90.00 |
Refinement procedure
| Resolution | 33.950 - 2.636 |
| R-factor | 0.2396 |
| Rwork | 0.239 |
| R-free | 0.25950 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.880 |
| Data reduction software | autoPROC |
| Data scaling software | autoPROC |
| Phasing software | MOLREP |
| Refinement software | BUSTER (2.11.8) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 82.121 | 2.958 |
| High resolution limit [Å] | 2.636 | 2.636 |
| Rpim | 0.056 | |
| Number of reflections | 16610 | 830 |
| <I/σ(I)> | 11.3 | |
| Completeness [%] | 92.3 | 68.7 |
| Redundancy | 11.4 | 12 |
| CC(1/2) | 0.999 | 0.679 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293.15 | 27%PEG3350, 0.1M Bis-Tris |
