9GWJ

Crystal structure of CINP-c1orf109 complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-10-15
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.979
Spacegroup name	P 21 21 21
Unit cell lengths	82.874, 115.166, 148.985
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.920 - 3.690
R-factor	0.2667
Rwork	0.265
R-free	0.29800
Structure solution method	SAD
RMSD bond length	0.002
RMSD bond angle	0.437
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	CRANK2
Refinement software	PHENIX (1.21.2_5419)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.920	3.820
High resolution limit [Å]	3.690	3.690
Rmerge	0.411	6.252
Number of reflections	15894	1552
<I/σ(I)>	8.277	0.665
Completeness [%]	99.8	98.9
Redundancy	25.3	17.29
CC(1/2)	0.999	0.176

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7	277.15	0.236M sodium citrate, 23.4% 2-propanol, 0.1M sodium cacodylate pH 7