9GTG

RIPK1 in complex with AZ"902

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	MAX IV BEAMLINE BioMAX
Synchrotron site	MAX IV
Beamline	BioMAX
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-03-10
Detector	DECTRIS PILATUS 200K
Wavelength(s)	0.976
Spacegroup name	P 21 21 21
Unit cell lengths	47.084, 96.491, 129.002
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	77.270 - 2.250
R-factor	0.22118
Rwork	0.217
R-free	0.29485
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.497
Data scaling software	Aimless
Phasing software	MOLREP
Refinement software	REFMAC (5.8.0352)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	77.270	2.395
High resolution limit [Å]	2.250	2.255
Rmerge	0.109	1.459
Rmeas	0.119	1.576
Rpim	0.046	0.591
Total number of observations		8545
Number of reflections	24404	1220
<I/σ(I)>	9	1.3
Completeness [%]	85.6
Redundancy	6.7	7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	20 % PEG4000, 0.3 M NaCl, 0.1 M MES pH 6.5.